有機化學實驗 (王紅) 王紅 梁仁校 強根榮 9787122445513 【台灣高等教育出版社】

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原出版社:化學工業
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書名:有機化學實驗 (王紅)
ISBN:9787122445513
出版社:化學工業
著編譯者:王紅 梁仁校 強根榮
頁數:235
所在地:中國大陸 *此為代購商品
書號:1626583
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內容簡介

《有機化學實驗(雙語版)》全書共6章,分別為:有機化學實驗的一般知識、有機化學實驗的基本操作、有機化學基礎性實驗、有機化學綜合性實驗、研究性文獻實驗和典型實驗的學習指導。本書在立足基本能力培養的同時,還補充完善了新型的有機合成技術和綜合性實驗內容,以實現知識、能力的傳承與創新協調發展。結合雙語實驗教學的特點和存在的問題,本書以英文為主,中文為輔,以期給讀者提供一個相對完整的專業英語的學習環境,提升其專業英語的閱讀、理解和書寫能力。 本書可作為化學、化學工程與工藝、應用化學、能源化學工程、安全工程、材料科學與工程、生物製藥、環境科學等專業的雙語教學配套實驗教材,也可供留學生和相關專業人員參考。

目錄

Chapter 1 Introduction of Experimental Organic Chemistry
1 1 The Role of Experimental Organic Chemistry
1 2 General Rules for the Organic Chemistry Experiments
1 3 Safety in the Organic Chemistry Laboratory
1 4 Pre-lab Reports Notebooks and Lab Reports in the Laboratory
1 5 Common Laboratory Glassware and Equipment
1 6 The Literature of Organic Chemistry
1 7 Green Chemistry in the Organic Laboratory
Chapter 2 Basic Operations of Organic Chemistry Experiments
2 1 Heating and Cooling
2 2 Drying Organic Solutions and Solids
2 3 Filtration
2 4 Simple Distillation and Boiling Point
2 5 Fractional Distillation
2 6 Steam Distillation
2 7 Vacuum Distillation
2 8 Extraction and Washing
2 9 Recrystallization
2 10 Sublimation
2 11 Measurement of the Melting Point
2 12 Refluxing
2 13 Stirring Methods
2 14 Water-free and Air-free Operation
2 15 Chromatography Techniques
Chapter 3 Fundamental Experiments
3 1 Unsaturated Hydrocarbons
Exp 1 Preparation of Cyclohexene
Exp 2 Preparation of Phenylacetylene
3 2 Alkyl Halides
Exp 3 Preparation of 1-Bromobutane
Exp 4 Preparation of 2 Chloro 2 methylbutane
3 3 Alcohols,Phenols and Ethers
Exp 5 Preparation of 2-Methyl-2-butanol
Exp 6 Preparation of Triphenylmethanol
Exp 7 Preparation of Di n-butyl Ether
Exp 8 Preparation of Ethyl Phenyl Ether
Exp 9 Preparation of o-tert Butylhydroquinone
3 4 Aldehydes and Ketones
Exp 10 Preparation of Cyclohexanone
Exp 11 Preparation of Acetophenone
Exp 12 Preparation of Benzaldehyde
3 5 Carboxylic Acids
Exp 13 Preparation of Benzoic Acid
Exp 14 Preparation of Cinnamic Acid
Exp 15 Preparation of Hexane-1,6 dionic Acid
3 6 Carboxylic Acid Derivatives
Exp 16 Preparation of Ethyl Acetate
Exp 17 Preparation of nDibutyl Phthalate
3 7 Nitrogen-containing Compounds
Exp 18 Preparation of Acetanilide
Exp 19 Preparation of Methyl Orange
3 8 Heterocyclic Compounds
Exp 20 Preparation of 8-Hydroxyquinoline
Exp 21 Extraction and Separation of Caffeine from Tea Leaves
Chapter 4 Comprehensive Experiments
Exp 1 Preparation of Benzyl Alcohol and Benzoic Acid
Exp 2 Preparation of Benzil and Thin-layer Chromatography
Exp 3 Preparation of Acetylferrocene and Column Chromatography
Exp 4 Preparation of Ethyl Acetoacetate by the Claisen Condensation Reaction
Exp 5 Synthesis and Characterization of Aspirin
Exp 6 Multi-step Synthesis of Sulfanilamide
Exp 7 A Solvent Free Cannizzaro Reaction and Thin-layer Chromatography
Exp 8 Preparation of 4-Vinylbenzoic Acid by a Wittig Reaction
Exp 9 Preparation of Dimedone via the Robinson Annulation
Exp 10 Preparation of Cinnamic Acid by the Knoevenagel Condensation
Exp 11 Microwave assisted Preparation of Benzoic Acid and Ethyl Benzoate
Chapter 5 Experiments from Research and Literature
Exp 1 Synthesis of 3-Substituted Isoindolin-1-ones by Solvent-free Grinding Reaction
Exp 2 Electroorganic Synthesis of Nitriles
Exp 3 Ultrasonic Assisted Green Protocol for the Synthesis of N,N-bis Phenylsulfamide
Exp 4 Clean Synthesis in Water:Uncatalysed Preparation of Ylidenemalononitriles
Exp 5 Transition metal-catalyzed Convenient Synthesis of Internal Alkyne
Exp 6 N-Heterocyclic Carbene Catalyzed Intramolecular Benzoin Condensation to Access 9,10-Phenanthraquinone
Exp 7 Optical Resolution of (★)(S)-Methyl-(S)phenylsulfoximine with (+)-L-Camphorsulfonic Acid
Exp 8 Synthesis of Benzyl Acetate in Room Temperature lonic Liquids
Exp 9 Green Synthesis of 4-Bromoaniline
Exp 10 Pinacol Rearrangement and Photochemical Synthesis of Benzopinacol
Chapter 6 Study Guide of Some Typical Experiments
Exp 1 Preparation of Cyclohexene (Miniscale Reaction)
Exp 2 Preparation of 1
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